3. Секція "Матеріалознавство порошкових та композиційних матеріалів і покриттів"
Постійне посилання на фондhttps://archive.ipms.kyiv.ua/handle/123456789/23
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Документ POLYMER MATERIALS REINFORCED WITH SILICON NITRIDE PARTICLES FOR 3D PRINTING(Springer Science+Business Media, LLC, 2020) O.B. Zgalat-Lozynskyy; O.O. Matviichuk; O.I.Tolochyn; O.V. Ievdokymova; N.O. Zgalat-Lozynska; V.I.Zakiev3Comprehensive research into the production of a ceramic-reinforced polymer material from highdensity polyethylene or polypropylene and -Si3N4 powder was conducted. The incorporation of silicon nitride ceramic particles (5 and 10 vol.%) into the polymers to make polymer–ceramic filaments was studied step by step. High-quality polypropylene–ceramic filaments could be obtained at an extrusion temperature of 150oC with an extrusion speed of 20 cm/min and polyethylene–ceramic filaments at 160oC and 30 cm/min. Data on the shape and size distribution of Si3N4 particles were used to simulate the elementary volume of the filaments to determine the mechanical properties of the composites applying a 2D finite-element model. The reinforcement of the polypropylene/polyethylene-matrix material by 10 vol.% Si3N4 particles was not sufficient because the composite elastic modulus increased insignificantly and the critical strain decreased substantially to incorporate a greater volume of hard particles to improve the elastic modulus. To assess the quality of the polymer–ceramic filaments, parts of different shape (washer and auger) from reinforced and unreinforced filaments were designed and printed. The printed polymer–ceramic parts demonstrated a smooth surface and had no ledges or discontinuous areas. The mechanical (Vickers and Brinell hardness) and tribological (volume wear) properties of the materials were examined. Wear tests of the polyethylene–Si3N4 composite showed that its wear resistance tended to improve with increasing ceramic content of the filament. The low abrasive wear of the Si3N4-reinforced polypropylene/polyethylene material and the behavior of ceramic particles in contact with the indenter indicate that the composite has high fracture resistance in 3D printing.Документ Exploration of Titanium-Based Fine-Particle Additive Influence on Cohesive and Adhesive Strength Enhancement in Epoxy-Polymer Composites(PHYSICS AND CHEMISTRY OF SOLID STATE, 2024) O. Baranovska; G. Bagliuk; A. Buketov; O. Sapronov; D. BaranovskyiThe study examines how the inclusion of a dispersed powder filler affects the physico-mechanical properties of an ultrasound-modified epoxy matrix. Varying the filler content from 5 % to 60 % by weight in the composite revealed an optimal concentration for enhanced mechanical properties. Introducing the filler at 5 % led to maximum impact strength (W = 18.47 kJ/m2 ) and minimized destructive stresses during bending (σB = 51.75 MPa). At 10 % filler concentration, destructive bending stresses increased significantly from σB = 48.0 MPa to σB= 74.85 MPa, with impact strength improving from W = 7.4 kJ/m2 to W = 17.42...18.47 kJ/m2. Further increasing filler content to 20 - 60 % resulted in a slight decrease in destructive stresses while still surpassing for the filler-free epoxy matrix strength. Optimal modifier content improved adhesive characteristics, achieving a peak adhesive strength (σa = 33.4 MPa) at 20 % filler, albeit with residual stresses at 0.34 MPa. Introducing the modifier at 10% increased adhesive strength to σa = 28.6 MPa, marking a 1.15-fold improvement over the filler-free epoxy matrix, while reducing residual stresses from σres = 1.4 MPa to σres = 1.0 MPa. Higher filler content (40 - 60 %) led to decreased adhesive strength and increased residual stresses (σres = 0.62...0.69 MPa).